I am attempting to pattern Cr/Au films on Pyrex by liftoff. However the I am
getting unacceptable results due to poor adhesion of the liftoff resist.
my process is as follows:
Clean Pyrex in Piranha, DI rinse, blow dry.
Dehydration bake 30 minutes ~ 200 degC
Spin on Microposit LOR 10A
Bake 30 min 150-190 degC
Spin on S1813 resist
Bake 30 min at 90 degC
Expose and develop
Bake 30 min at 90 degC (to avoid outgassing during sputter)
Sputter 100A Cr + 1 Micron Au
My understanding was that HMDS prime isn't necessary prior to application of LOR
or LOL. I had good results with the above process on Si.
Would a HMDS prime improve LOR adhesion to Pyrex? If so what is an ideal prime
e.g. resulting contact angle for water drop?
Is there some other technique to improve LOR/LOL adhesion to Pyrex?
Roger Shile